赵蒙, 周晖, 刘兴光, 等. 真空下载荷对a-C:H超润滑薄膜的摩擦学性能影响研究[J]. 真空与低温, 2021, 27(3): 224-230. DOI: 10.3969/j.issn.1006-7086.2021.03.004
引用本文: 赵蒙, 周晖, 刘兴光, 等. 真空下载荷对a-C:H超润滑薄膜的摩擦学性能影响研究[J]. 真空与低温, 2021, 27(3): 224-230. DOI: 10.3969/j.issn.1006-7086.2021.03.004
ZHAO Meng, ZHOU Hui, LIU Xingguang, et al. The Influence of Load on the Tribological Properties of a-C:H Based Super-lubricating Film in Vacuum Environment[J]. VACUUM AND CRYOGENICS, 2021, 27(3): 224-230. DOI: 10.3969/j.issn.1006-7086.2021.03.004
Citation: ZHAO Meng, ZHOU Hui, LIU Xingguang, et al. The Influence of Load on the Tribological Properties of a-C:H Based Super-lubricating Film in Vacuum Environment[J]. VACUUM AND CRYOGENICS, 2021, 27(3): 224-230. DOI: 10.3969/j.issn.1006-7086.2021.03.004

真空下载荷对a-C:H超润滑薄膜的摩擦学性能影响研究

The Influence of Load on the Tribological Properties of a-C:H Based Super-lubricating Film in Vacuum Environment

  • 摘要: 高含H量a-C:H薄膜因能在宏观尺度实现超润滑(μ< 0.01)而备受关注,具有广阔的应用前景。但高含H量a-C:H薄膜的摩擦学特性对测试条件十分敏感,为此,本文研究了典型工况(载荷)对薄膜摩擦学特性的影响及其摩擦学机制。采用球盘摩擦实验机对a-C:H薄膜在不同载荷下进行摩擦实验;使用表面轮廓仪观测薄膜在不同工况下的磨损形貌,计算磨损率;使用拉曼光谱仪测试摩擦界面处碳相结构信息及H元素的相对含量。结果表明:随着载荷的增加,摩擦界面处sp3键向sp2键转化程度增加,sp2键石墨化程度增加;摩擦界面处H元素的消耗速率增加,消耗的不均匀性同时增加;在超润滑阶段,摩擦因数基本不受载荷影响,薄膜的耐磨性能依赖于超润滑状态带来的超低摩擦因数,不同载荷下薄膜均没有明显磨损;超出超润滑阶段后,薄膜均出现较严重磨损。

     

    Abstract: The a-C:H-based films have attracted great attention because of its ability to achieve super-lubrication at macro-scale,resulting in broad application prospects.However,the tribological characteristics of a-C:H-based films are very sensitive to the test conditions.In this study the influence of a typical working condition,normal load,on the film's tribological properties,and the underlying mechanism were studied.A ball-disk friction test machine was used to conduct friction experiments on the film under different loads.The wear morphology and volume under different testing conditions were measured using an optical profilometer.Raman spectroscopy was used to reveal the carbon phase structure informa-tion at the wear scar.The results showed that with the increase of normal load,the conversion of sp3bond to sp2bond at the wear scar increased,and the degree of graphitization of sp2bond increased,the hydrogen consumption rate at the wear scar increased with increased normal load as well.In the super lubrication stage,the load showed very limited effect on the frictional performance of the film.The wear resistance of the film relied highly on the ultra-low friction coefficient.No ob-vious wear was observed in all working conditions during the super-lubrication stage.Once the super-lubrication stage ter-minated due to hydrogen efficiency,severe wear started to appear,resulting in much higher wear vote.

     

/

返回文章
返回