付学成, 瞿敏妮, 权雪玲, 等. 电子束蒸镀快速沉积铜膜研究[J]. 真空与低温, 2023, 29(1): 5-11. DOI: 10.3969/j.issn.1006-7086.2023.01.002
引用本文: 付学成, 瞿敏妮, 权雪玲, 等. 电子束蒸镀快速沉积铜膜研究[J]. 真空与低温, 2023, 29(1): 5-11. DOI: 10.3969/j.issn.1006-7086.2023.01.002
FU Xuecheng, QU Minni, QUAN Xueling, et al. Rapid Deposition of Copper Film by Electron Beam Evaperation[J]. VACUUM AND CRYOGENICS, 2023, 29(1): 5-11. DOI: 10.3969/j.issn.1006-7086.2023.01.002
Citation: FU Xuecheng, QU Minni, QUAN Xueling, et al. Rapid Deposition of Copper Film by Electron Beam Evaperation[J]. VACUUM AND CRYOGENICS, 2023, 29(1): 5-11. DOI: 10.3969/j.issn.1006-7086.2023.01.002

电子束蒸镀快速沉积铜膜研究

Rapid Deposition of Copper Film by Electron Beam Evaperation

  • 摘要: 利用电子束蒸镀设备沉积金属薄膜是微电子领域最常见的薄膜沉积工艺之一。然而使用普通钨坩埚电子束蒸镀铜薄膜时,沉积速度非常低。这是因为熔融的铜与钨坩埚是浸润的,当提高电子枪功率时,液态铜的表面自由能随着温度的升高而降低,液态铜会沿着坩埚壁向上铺展,消耗电子束能量。为此,对钨衬埚壁进行结构优化,阻止了电子枪功率较高时液态铜的向上铺展,将铜膜的沉积速度从2 Å/s提高到20 Å/s,并对不同沉积速率制备的铜薄膜的粗糙度、均匀性、应力进行对比,验证了该方法的可行性。

     

    Abstract: Deposition of metal films by electron beam evaporation equipment is one of the most common processes in the field of microelectronics fabrication.However, when using ordinary tungsten crucible to evaporate copper films, the evaporation speed is very low.This is because the molten copper and tungsten crucibles are wetted, hence, when the power of the electron gun is increased, the surface free energy of liquid copper decreases with temperature increasing, and the melted copper will consume the energy of the electron beam to spread upward along the crucible wall.Therefore, we opti-mized the structure of the turgsten crulible wall to prevent the liquid copper from spreading upward and doing work when the electron beam power increased, and increased the deposition rate of the copper film from 2 Å/s to 20 Å/s.Meanwhile, the roughness, uniformity and stress of copper films prepared at different deposition rates were compared to verify the feasibility of the method.

     

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