电子束重熔处理对硅化物涂层表面形貌和性能的影响
EFFECT OF ELECTRON BEAM RE-MELTING ON SURFACE MOTPHOLOGY AND PROPERTIES OF SILICIDE COATING
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摘要: 在Nb521铌合金表面采用料浆烧结法制备硅化物涂层,利用高频扫描电子束对硅化物涂层进行重熔处理,通过扫描电子显微镜对处理样品表面形貌进行组织结构分析。研究表明,经过电子束重熔处理,硅化物涂层表面陶瓷晶粒粒度降低,表面粗糙度降低,陶瓷颗粒之间烧结作用增强,重熔区域与未处理区域具有明显的边界,电子束能量分布较均匀。电子束重熔增强了陶瓷涂层的烧结作用,涂层致密度增加,硅化物层的抗氧化性能和抗热震性能提高。Abstract: The silicide coating was prepared by fused slurry method on Nb521 alloy,the silicide coating was re-melted by high frequency electron beam,the morphology of specimen was analyzed by SEM.It is found that after electron beam re-melt process,the surface ceramic grain granularity and surface roughness decrease,the sintering effect between ceramic grains increased,the obvious boundary was found between primary region and region re-melted,it prove that the energy distributing is well-proportioned.The silicide coating’ sintering effect increased after EB re-melting process,and the coating became dense,the surface roughness of coating decrease,the high-temperature oxidation resistance and shock testing validate capability improved.